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Ticket #3715: Angew 04-20.cif

File Angew 04-20.cif, 90.5 KB (added by ubaumann@…, 5 years ago)
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Line
1
2	data_TGDH
3
4	_audit_creation_method 'SHELXL-2018/3'
5	_shelx_SHELXL_version_number '2018/3'
6	_chemical_name_systematic ?
7	_chemical_name_common ?
8	_chemical_melting_point ?
9	_chemical_formula_moiety
10	'C6 H11 N3 O4, 2(H2 O)'
11	_chemical_formula_sum
12	'C6 H15 N3 O6'
13	_chemical_formula_weight 225.21
14
15	loop_
16	_atom_type_symbol
17	_atom_type_description
18	_atom_type_scat_dispersion_real
19	_atom_type_scat_dispersion_imag
20	_atom_type_scat_source
21	'C' 'C' 0.0181 0.0091
22	'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
23	'H' 'H' 0.0000 0.0000
24	'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
25	'N' 'N' 0.0311 0.0180
26	'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
27	'O' 'O' 0.0492 0.0322
28	'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
29
30	_space_group_crystal_system orthorhombic
31	_space_group_IT_number 29
32	_space_group_name_H-M_alt 'P c a 21'
33	_space_group_name_Hall 'P 2c -2ac'
34
35	_shelx_space_group_comment
36	;
37	The symmetry employed for this shelxl refinement is uniquely defined
38	by the following loop, which should always be used as a source of
39	symmetry information in preference to the above space-group names.
40	They are only intended as comments.
41	;
42
43	loop_
44	_space_group_symop_operation_xyz
45	'x, y, z'
46	'-x, -y, z+1/2'
47	'x+1/2, -y, z'
48	'-x+1/2, y, z+1/2'
49
50	_cell_length_a 21.499(2)
51	_cell_length_b 9.8041(9)
52	_cell_length_c 4.7683(3)
53	_cell_angle_alpha 90
54	_cell_angle_beta 90
55	_cell_angle_gamma 90
56	_cell_volume 1005.05(15)
57	_cell_formula_units_Z 4
58	_cell_measurement_temperature 173(2)
59	_cell_measurement_reflns_used 490
60	_cell_measurement_theta_min 4.1020
61	_cell_measurement_theta_max 72.2490
62
63	_exptl_crystal_description needles
64	_exptl_crystal_colour Colourless
65	_exptl_crystal_density_meas ?
66	_exptl_crystal_density_method ?
67	_exptl_crystal_density_diffrn 1.488
68	_exptl_crystal_F_000 480
69	_exptl_transmission_factor_min ?
70	_exptl_transmission_factor_max ?
71	_exptl_crystal_size_max 0.450
72	_exptl_crystal_size_mid 0.027
73	_exptl_crystal_size_min 0.010
74	_exptl_absorpt_coefficient_mu 1.151
75	_shelx_estimated_absorpt_T_min ?
76	_shelx_estimated_absorpt_T_max ?
77	_exptl_absorpt_correction_type analytical
78	_exptl_absorpt_correction_T_min 0.834
79	_exptl_absorpt_correction_T_max 0.989
80	_exptl_absorpt_process_details
81	;
82	CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015)
83	Analytical numeric absorption correction using a multifaceted crystal
84	model based on expressions derived by R.C. Clark & J.S. Reid.
85	(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
86	Empirical absorption correction using spherical harmonics,
87	implemented in SCALE3 ABSPACK scaling algorithm.
88	;
89	_exptl_absorpt_special_details ?
90	_diffrn_ambient_temperature 173(2)
91	_diffrn_radiation_wavelength 1.54184
92	_diffrn_radiation_type CuK\a
93	_diffrn_source 'Enhance Ultra (Cu) X-ray Source'
94	_diffrn_measurement_device_type 'Agilent Xcalibur PX Ultra A'
95	_diffrn_measurement_method 'omega scans'
96	_diffrn_detector_area_resol_mean 10.4115
97	_diffrn_reflns_number 2076
98	_diffrn_reflns_av_unetI/netI 0.0710
99	_diffrn_reflns_av_R_equivalents 0.0470
100	_diffrn_reflns_limit_h_min -25
101	_diffrn_reflns_limit_h_max 26
102	_diffrn_reflns_limit_k_min -12
103	_diffrn_reflns_limit_k_max 11
104	_diffrn_reflns_limit_l_min -5
105	_diffrn_reflns_limit_l_max 5
106	_diffrn_reflns_theta_min 4.113
107	_diffrn_reflns_theta_max 73.301
108	_diffrn_reflns_theta_full 67.684
109	_diffrn_measured_fraction_theta_max 0.955
110	_diffrn_measured_fraction_theta_full 0.977
111	_diffrn_reflns_Laue_measured_fraction_max 0.955
112	_diffrn_reflns_Laue_measured_fraction_full 0.977
113	_diffrn_reflns_point_group_measured_fraction_max 0.674
114	_diffrn_reflns_point_group_measured_fraction_full 0.696
115	_reflns_number_total 1350
116	_reflns_number_gt 1056
117	_reflns_threshold_expression 'I > 2\s(I)'
118	_reflns_Friedel_coverage 0.248
119	_reflns_Friedel_fraction_max 0.308
120	_reflns_Friedel_fraction_full 0.330
121
122	_reflns_special_details
123	;
124	Reflections were merged by SHELXL according to the crystal
125	class for the calculation of statistics and refinement.
126
127	_reflns_Friedel_fraction is defined as the number of unique
128	Friedel pairs measured divided by the number that would be
129	possible theoretically, ignoring centric projections and
130	systematic absences.
131	;
132
133	_computing_data_collection 'CrysAlisPro, Rigaku OD'
134	_computing_cell_refinement 'CrysAlisPro, Rigaku OD'
135	_computing_data_reduction 'CrysAlisPro, Rigaku OD'
136	_computing_structure_solution 'SHELXS-2014 (Sheldrick, 2017)'
137	_computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)'
138	_computing_molecular_graphics 'Bruker SHELXTL'
139	_computing_publication_material 'CIFTAB-2014 (Sheldrick, 2017)'
140	_refine_special_details ?
141	_refine_ls_structure_factor_coef Fsqd
142	_refine_ls_matrix_type full
143	_refine_ls_weighting_scheme calc
144	_refine_ls_weighting_details
145	'w=1/[\s^2^(Fo^2^)+(0.0611P)^2^] where P=(Fo^2^+2Fc^2^)/3'
146	_atom_sites_solution_primary ?
147	_atom_sites_solution_secondary ?
148	_atom_sites_solution_hydrogens mixed
149	_refine_ls_hydrogen_treatment mixed
150	_refine_ls_extinction_method none
151	_refine_ls_extinction_coef .
152	_refine_ls_abs_structure_details
153	;
154	Classical Flack method preferred over Parsons because s.u. lower.
155	;
156	_refine_ls_abs_structure_Flack -0.8(6)
157	_chemical_absolute_configuration .
158	_refine_ls_number_reflns 1350
159	_refine_ls_number_parameters 172
160	_refine_ls_number_restraints 10
161	_refine_ls_R_factor_all 0.0693
162	_refine_ls_R_factor_gt 0.0508
163	_refine_ls_wR_factor_ref 0.1271
164	_refine_ls_wR_factor_gt 0.1149
165	_refine_ls_goodness_of_fit_ref 1.011
166	_refine_ls_restrained_S_all 1.007
167	_refine_ls_shift/su_max 0.001
168	_refine_ls_shift/su_mean 0.000
169
170	loop_
171	_atom_site_label
172	_atom_site_type_symbol
173	_atom_site_fract_x
174	_atom_site_fract_y
175	_atom_site_fract_z
176	_atom_site_U_iso_or_equiv
177	_atom_site_adp_type
178	_atom_site_occupancy
179	_atom_site_site_symmetry_order
180	_atom_site_calc_flag
181	_atom_site_refinement_flags_posn
182	_atom_site_refinement_flags_adp
183	_atom_site_refinement_flags_occupancy
184	_atom_site_disorder_assembly
185	_atom_site_disorder_group
186	C1 C 0.1229(2) 0.8799(5) 0.1816(12) 0.0287(10) Uani 1 1 d . . . . .
187	O2 O 0.07424(14) 0.8109(4) 0.1740(9) 0.0296(7) Uani 1 1 d . . . . .
188	O3 O 0.13336(15) 0.9747(3) 0.3573(10) 0.0355(8) Uani 1 1 d . . . . .
189	C4 C 0.1758(2) 0.8509(5) -0.0267(12) 0.0276(10) Uani 1 1 d . . . . .
190	H4A H 0.174337 0.919257 -0.179434 0.033 Uiso 1 1 calc R U . . .
191	H4B H 0.216181 0.860964 0.070891 0.033 Uiso 1 1 calc R U . . .
192	N5 N 0.17191(17) 0.7145(4) -0.1479(5) 0.0265(9) Uani 1 1 d D . . . .
193	H5 H 0.1744(17) 0.708(3) -0.3359(7) 0.018(12) Uiso 1 1 d D . . . .
194	C6 C 0.1776(2) 0.6059(5) 0.0195(12) 0.0263(10) Uani 1 1 d . . . . .
195	O6 O 0.18295(17) 0.6145(4) 0.2753(9) 0.0346(9) Uani 1 1 d . . . . .
196	C7 C 0.1774(2) 0.4669(5) -0.1249(12) 0.0281(10) Uani 1 1 d . . . . .
197	H7A H 0.160073 0.476081 -0.316427 0.034 Uiso 1 1 calc R U . . .
198	H7B H 0.220516 0.432494 -0.141082 0.034 Uiso 1 1 calc R U . . .
199	N8 N 0.14004(17) 0.3702(4) 0.0351(8) 0.0299(9) Uani 1 1 d D . . . .
200	H8 H 0.1601(4) 0.3158(7) 0.1571(13) 0.033(14) Uiso 1 1 d D . . . .
201	C9 C 0.0784(2) 0.3693(5) 0.0133(12) 0.0243(9) Uani 1 1 d . . . . .
202	O9 O 0.04878(15) 0.4400(3) -0.1534(9) 0.0314(8) Uani 1 1 d . . . . .
203	C10 C 0.0451(2) 0.2742(5) 0.2152(11) 0.0291(11) Uani 1 1 d . . . . .
204	H10A H 0.057766 0.178749 0.178007 0.035 Uiso 1 1 calc R U . . .
205	H10B H 0.056789 0.296980 0.410461 0.035 Uiso 1 1 calc R U . . .
206	N11 N -0.02269(15) 0.2879(3) 0.1797(4) 0.0271(8) Uani 1 1 d D . . . .
207	H11A H -0.0339(6) 0.2512(10) 0.0142(9) 0.049(19) Uiso 1 1 d D . . . .
208	H11B H -0.0343(6) 0.3758(4) 0.196(8) 0.035(15) Uiso 1 1 d D . . . .
209	H11C H -0.0438(4) 0.2358(7) 0.3025(12) 0.06(2) Uiso 1 1 d D . . . .
210	O20 O 0.21576(13) 0.1805(3) 0.3546(6) 0.0346(8) Uani 1 1 d D . . . .
211	H20A H 0.1933(3) 0.1033(5) 0.342(10) 0.049(18) Uiso 1 1 d D . . . .
212	H20B H 0.2376(3) 0.185(5) 0.5154(9) 0.049(19) Uiso 1 1 d D . . . .
213	O30 O 0.04175(12) 0.0382(4) 0.7492(6) 0.0399(9) Uani 1 1 d D . . . .
214	H30A H 0.0717(2) 0.0205(19) 0.6226(12) 0.038(17) Uiso 1 1 d D . . . .
215	H30B H 0.0058(2) 0.053(2) 0.6576(16) 0.046(18) Uiso 1 1 d D . . . .
216
217	loop_
218	_atom_site_aniso_label
219	_atom_site_aniso_U_11
220	_atom_site_aniso_U_22
221	_atom_site_aniso_U_33
222	_atom_site_aniso_U_23
223	_atom_site_aniso_U_13
224	_atom_site_aniso_U_12
225	C1 0.034(2) 0.035(2) 0.017(2) -0.002(2) -0.002(2) 0.001(2)
226	O2 0.0275(16) 0.0395(16) 0.0218(17) -0.0008(17) 0.0004(16) -0.0025(14)
227	O3 0.0362(17) 0.0424(18) 0.0278(18) -0.0105(19) 0.0050(18) -0.0027(15)
228	C4 0.029(2) 0.031(2) 0.023(2) 0.001(2) 0.0008(19) 0.0000(19)
229	N5 0.0280(19) 0.035(2) 0.0170(19) 0.0030(19) -0.0003(18) 0.0004(15)
230	C6 0.023(2) 0.035(2) 0.020(3) 0.002(2) 0.0037(19) 0.0007(19)
231	O6 0.044(2) 0.0421(18) 0.0172(19) 0.0017(16) -0.0018(15) 0.0012(16)
232	C7 0.028(2) 0.034(2) 0.022(2) -0.002(2) 0.008(2) -0.0026(18)
233	N8 0.029(2) 0.036(2) 0.024(2) 0.0054(19) 0.002(2) 0.0021(18)
234	C9 0.027(2) 0.032(2) 0.013(2) -0.0009(19) -0.0009(19) -0.001(2)
235	O9 0.0334(16) 0.0367(16) 0.0243(18) 0.0064(19) -0.0007(16) 0.0040(14)
236	C10 0.030(2) 0.037(2) 0.020(3) 0.002(2) -0.001(2) -0.0019(19)
237	N11 0.0283(19) 0.034(2) 0.0189(19) -0.0001(19) 0.0008(18) -0.0036(16)
238	O20 0.0382(18) 0.0376(17) 0.0281(17) 0.0056(18) -0.0060(19) -0.0028(15)
239	O30 0.0390(19) 0.060(2) 0.0207(18) 0.0002(19) -0.0001(16) 0.0109(17)
240
241	_geom_special_details
242	;
243	All esds (except the esd in the dihedral angle between two l.s. planes)
244	are estimated using the full covariance matrix. The cell esds are taken
245	into account individually in the estimation of esds in distances, angles
246	and torsion angles; correlations between esds in cell parameters are only
247	used when they are defined by crystal symmetry. An approximate (isotropic)
248	treatment of cell esds is used for estimating esds involving l.s. planes.
249	;
250
251	loop_
252	_geom_bond_atom_site_label_1
253	_geom_bond_atom_site_label_2
254	_geom_bond_distance
255	_geom_bond_site_symmetry_2
256	_geom_bond_publ_flag
257	C1 O2 1.246(6) . ?
258	C1 O3 1.271(6) . ?
259	C1 C4 1.536(7) . ?
260	C4 N5 1.460(6) . ?
261	N5 C6 1.336(6) . ?
262	C6 O6 1.228(7) . ?
263	C6 C7 1.528(7) . ?
264	C7 N8 1.457(6) . ?
265	N8 C9 1.329(6) . ?
266	C9 O9 1.233(6) . ?
267	C9 C10 1.520(7) . ?
268	C10 N11 1.474(6) . ?
269
270	loop_
271	_geom_angle_atom_site_label_1
272	_geom_angle_atom_site_label_2
273	_geom_angle_atom_site_label_3
274	_geom_angle
275	_geom_angle_site_symmetry_1
276	_geom_angle_site_symmetry_3
277	_geom_angle_publ_flag
278	O2 C1 O3 124.4(5) . . ?
279	O2 C1 C4 120.1(4) . . ?
280	O3 C1 C4 115.5(4) . . ?
281	N5 C4 C1 112.5(4) . . ?
282	C6 N5 C4 119.2(4) . . ?
283	O6 C6 N5 123.2(5) . . ?
284	O6 C6 C7 120.6(5) . . ?
285	N5 C6 C7 116.2(4) . . ?
286	N8 C7 C6 110.2(4) . . ?
287	C9 N8 C7 120.8(4) . . ?
288	O9 C9 N8 124.2(4) . . ?
289	O9 C9 C10 120.7(4) . . ?
290	N8 C9 C10 115.1(4) . . ?
291	N11 C10 C9 109.7(4) . . ?
292
293	loop_
294	_geom_hbond_atom_site_label_D
295	_geom_hbond_atom_site_label_H
296	_geom_hbond_atom_site_label_A
297	_geom_hbond_distance_DH
298	_geom_hbond_distance_HA
299	_geom_hbond_distance_DA
300	_geom_hbond_angle_DHA
301	_geom_hbond_site_symmetry_A
302	_geom_hbond_publ_flag
303	N5 H5 O6 0.9000(2) 2.079(14) 2.930(5) 157(3) 1_554 yes
304	N8 H8 O20 0.9000(1) 2.019(5) 2.904(4) 167.3(8) . yes
305	N11 H11A O2 0.9000(1) 1.938(6) 2.826(5) 168.3(14) 2_564 yes
306	N11 H11B O9 0.9000(1) 1.968(13) 2.839(4) 162(4) 2_565 yes
307	N11 H11C O2 0.9000(1) 1.943(6) 2.779(5) 153.8(7) 2_565 yes
308	O20 H20A O3 0.9000(2) 1.804(7) 2.685(4) 166(2) 1_545 yes
309	O20 H20B O20 0.9000(2) 1.904(4) 2.802(3) 176(4) 4 yes
310	O30 H30A O3 0.9000(1) 1.886(5) 2.785(5) 177.3(18) 1_545 yes
311	O30 H30B O2 0.9000(1) 2.180(13) 2.921(4) 139.2(16) 2_565 yes
312	O30 H30B O30 0.9000(1) 2.372(13) 3.077(4) 135.2(15) 2_554 yes
313
314	_refine_diff_density_max 0.222
315	_refine_diff_density_min -0.242
316	_refine_diff_density_rms 0.059
317
318	_shelx_res_file
319	;
320	TITL JH1902b in Pca2(1)
321	JH1902b.res
322	created by SHELXL-2018/3 at 08:28:19 on 20-Sep-2019
323	REM Pca2(1) (#29, found as P2(1)ca in -cba setting)
324	REM 50-2
325	CELL 1.54184 21.499126 9.804085 4.768275 90.0000 90.0000 90.0000
326	ZERR 4.00 0.002078 0.000872 0.000349 0.0000 0.0000 0.0000
327	LATT -1
328	SYMM -x,-y, z+1/2
329	SYMM x+1/2,-y, z
330	SYMM -x+1/2, y, z+1/2
331	SFAC C H N O
332	UNIT 24 60 12 24
333	TEMP -100
334
335	L.S. 6
336	FMAP 2
337	PLAN 10
338
339	ACTA
340
341	REM 'C6 H11 N3 O4, 2(H2 O)'
342	REM C6 H15 N3 O6
343
344	DFIX 0.9000 0.0001 N5 H5 N8 H8 N11 H11A N11 H11B N11 H11C
345	DFIX 0.9000 0.0001 O20 H20A O20 H20B O30 H30A O30 H30B
346
347	REM Instructions for potential hydrogen bonds
348	EQIV $1 x, y, z-1
349	EQIV $3 -x, -y+1, z-1/2
350	EQIV $4 -x, -y+1, z+1/2
351	EQIV $5 x, y-1, z
352	EQIV $6 -x+1/2, y, z+1/2
353	EQIV $7 -x, -y, z-1/2
354	HTAB N5 O6_$1
355	HTAB N8 O20
356	HTAB N11 O2_$3
357	HTAB N11 O9_$4
358	HTAB N11 O2_$4
359	HTAB O20 O3_$5
360	HTAB O20 O20_$6
361	HTAB O30 O3_$5
362	HTAB O30 O2_$4
363	HTAB O30 O30_$7
364
365	WGHT 0.061100
366	FVAR 3.67761
367	C1 1 0.122895 0.879912 0.181593 11.00000 0.03394 0.03499 =
368	0.01720 -0.00241 -0.00214 0.00096
369	O2 4 0.074239 0.810950 0.173963 11.00000 0.02746 0.03945 =
370	0.02180 -0.00084 0.00039 -0.00249
371	O3 4 0.133356 0.974662 0.357264 11.00000 0.03622 0.04236 =
372	0.02784 -0.01049 0.00498 -0.00268
373	C4 1 0.175792 0.850940 -0.026684 11.00000 0.02874 0.03069 =
374	0.02328 0.00093 0.00083 -0.00001
375	AFIX 23
376	H4A 2 0.174337 0.919257 -0.179434 11.00000 -1.20000
377	H4B 2 0.216181 0.860964 0.070891 11.00000 -1.20000
378	AFIX 0
379	N5 3 0.171913 0.714454 -0.147870 11.00000 0.02802 0.03452 =
380	0.01701 0.00305 -0.00034 0.00044
381	H5 2 0.174376 0.708492 -0.335891 11.00000 0.01781
382	C6 1 0.177609 0.605942 0.019511 11.00000 0.02327 0.03539 =
383	0.02029 0.00220 0.00370 0.00066
384	O6 4 0.182952 0.614477 0.275263 11.00000 0.04436 0.04210 =
385	0.01720 0.00172 -0.00180 0.00118
386	C7 1 0.177364 0.466854 -0.124935 11.00000 0.02778 0.03416 =
387	0.02226 -0.00204 0.00776 -0.00264
388	AFIX 23
389	H7A 2 0.160073 0.476081 -0.316427 11.00000 -1.20000
390	H7B 2 0.220516 0.432494 -0.141082 11.00000 -1.20000
391	AFIX 0
392	N8 3 0.140043 0.370242 0.035065 11.00000 0.02918 0.03628 =
393	0.02438 0.00543 0.00202 0.00208
394	H8 2 0.160131 0.315800 0.157100 11.00000 0.03301
395	C9 1 0.078438 0.369341 0.013339 11.00000 0.02741 0.03212 =
396	0.01336 -0.00091 -0.00092 -0.00111
397	O9 4 0.048783 0.440032 -0.153438 11.00000 0.03339 0.03666 =
398	0.02426 0.00635 -0.00072 0.00397
399	C10 1 0.045132 0.274156 0.215161 11.00000 0.02982 0.03728 =
400	0.02013 0.00239 -0.00085 -0.00190
401	AFIX 23
402	H10A 2 0.057766 0.178749 0.178007 11.00000 -1.20000
403	H10B 2 0.056789 0.296980 0.410461 11.00000 -1.20000
404	AFIX 0
405	N11 3 -0.022686 0.287949 0.179706 11.00000 0.02832 0.03418 =
406	0.01889 -0.00009 0.00079 -0.00358
407	H11A 2 -0.033854 0.251230 0.014205 11.00000 0.04885
408	H11B 2 -0.034348 0.375759 0.195966 11.00000 0.03461
409	H11C 2 -0.043787 0.235811 0.302517 11.00000 0.06104
410	O20 4 0.215756 0.180467 0.354637 11.00000 0.03819 0.03763 =
411	0.02806 0.00559 -0.00605 -0.00278
412	H20A 2 0.193286 0.103252 0.342122 11.00000 0.04937
413	H20B 2 0.237595 0.184731 0.515424 11.00000 0.04884
414	O30 4 0.041752 0.038200 0.749189 11.00000 0.03900 0.06001 =
415	0.02073 0.00022 -0.00007 0.01090
416	H30A 2 0.071739 0.020465 0.622634 11.00000 0.03789
417	H30B 2 0.005751 0.052634 0.657559 11.00000 0.04600
418
419	HKLF 4
420
421
422
423
424	REM JH1902b in Pca2(1)
425	REM wR2 = 0.1271, GooF = S = 1.011, Restrained GooF = 1.007 for all data
426	REM R1 = 0.0508 for 1056 Fo > 4sig(Fo) and 0.0693 for all 1350 data
427	REM 172 parameters refined using 10 restraints
428
429	END
430
431	WGHT 0.0611 0.0000
432
433	REM Highest difference peak 0.222, deepest hole -0.242, 1-sigma level 0.059
434	Q1 1 0.0623 0.5213 -0.1585 11.00000 0.05 0.22
435	Q2 1 0.2472 0.6342 0.3933 11.00000 0.05 0.22
436	Q3 1 0.1733 0.5673 -0.1364 11.00000 0.05 0.22
437	Q4 1 0.1373 0.1062 0.7055 11.00000 0.05 0.21
438	Q5 1 0.1254 1.0825 0.3590 11.00000 0.05 0.20
439	Q6 1 0.0380 0.1303 0.7521 11.00000 0.05 0.19
440	Q7 1 0.2208 0.2660 0.3557 11.00000 0.05 0.19
441	Q8 1 -0.0952 0.3600 0.1620 11.00000 0.05 0.19
442	Q9 1 0.1296 0.4435 -0.5159 11.00000 0.05 0.19
443	Q10 1 0.1726 1.0004 0.2576 11.00000 0.05 0.18
444	;
445	_shelx_res_checksum 33850
446
447	_shelx_hkl_file
448	;
449	0 0 -5 36.9016 94.3843 3
450	0 0 -4 89.4672 127.282 3
451	0 0 -3 9.84798 232.181 2
452	0 0 -2 66089.0 1607.28 2
453	0 0 -1 8.62788 146.853 2
454	0 -1 -5 36.3900 97.5311 3
455	0 -1 -4 4505.97 325.071 3
456	0 1 -4 4366.52 304.624 3
457	0 -1 -3 63.2288 228.266 2
458	0 -1 -2 14905.9 812.063 2
459	0 -1 -1 25.4481 170.637 2
460	0 1 0 5623.53 134.770 7
461	0 -2 -5 104.235 110.881 3
462	0 -2 -4 4541.50 323.009 3
463	0 -2 -4 3724.62 697.163 2
464	0 2 -4 4331.15 301.398 3
465	0 -2 -3 73.5953 235.434 2
466	0 -2 -2 24099.8 1101.71 2
467	0 2 0 2454.55 139.364 7
468	0 -3 -5 24.1777 93.5376 3
469	0 -3 -4 8348.31 417.530 3
470	0 -3 -3-407.955 289.801 2
471	0 -3 -2 1037.02 333.561 2
472	0 -3 -1 64.9024 151.263 1
473	0 3 0 8507.35 278.017 7
474	0 -4 -5-51.1849 80.2833 3
475	0 -4 -4 8640.46 425.271 3
476	0 -4 -3-433.616 228.948 2
477	0 -4 -2 25055.1 1309.05 2
478	0 -4 -1 62.9205 167.332 1
479	0 4 0 3790.00 227.241 7
480	0 4 3-42.7851 132.936 5
481	0 -5 -5-54.2159 72.1269 3
482	0 -5 -4 4567.22 321.288 3
483	0 -5 -3-36.9655 230.094 2
484	0 5 -1-232.219 122.706 7
485	0 -5 -1 87.2534 192.331 1
486	0 5 3-101.017 148.867 5
487	0 -6 -4 471.295 143.827 3
488	0 -6 -2 525.359 165.931 4
489	0 -6 -1 47.3596 246.360 1
490	0 -6 0 2013.69 370.897 1
491	0 6 2 787.826 174.519 5
492	0 6 3-53.3438 158.381 5
493	0 -7 -4 1452.03 178.629 3
494	0 -7 -2 4182.02 325.393 4
495	0 -7 -1-592.129 293.499 1
496	0 -7 0 6743.38 680.785 1
497	0 7 1 38.6754 140.115 5
498	0 7 2 4887.64 327.365 5
499	0 7 3-90.9297 143.557 5
500	0 -8 -4 3186.23 198.348 3
501	0 -8 -2 3264.27 300.906 4
502	0 -8 -1-35.0113 122.154 4
503	0 8 0 121.287 134.804 5
504	0 -8 0-313.720 255.218 1
505	0 -8 1-754.250 321.247 1
506	0 8 1 107.046 138.445 5
507	0 8 2 3693.72 303.385 5
508	0 8 3-76.1408 133.472 5
509	0 -9 -2 92.2199 135.873 4
510	0 -9 -1 20.3744 147.681 4
511	0 9 1-134.792 137.012 5
512	0 9 2 23.4804 140.537 5
513	0 9 3 26.2598 106.517 5
514	0 -10 -1-47.3052 131.529 4
515	0 10 1 149.027 139.242 5
516	0 10 2 1799.69 201.000 5
517	0 -11 -1-24.6563 99.5919 4
518	0 -11 0 3557.74 247.896 4
519	0 11 1 185.446 100.995 5
520	0 -12 0 3436.52 180.459 4
521	1 0 -5-30.0255 108.503 3
522	-1 0 -4-72.5413 120.191 3
523	1 0 -4 12.8710 126.278 3
524	1 0 -3 93.5241 245.115 2
525	-1 0 -3 119.212 230.725 2
526	-1 0 -2 165.992 225.295 2
527	1 0 -2-13.9257 207.302 2
528	-1 0 -1 47.0306 150.613 2
529	1 0 -1 0.48155 146.156 2
530	1 -1 -5 719.908 142.281 3
531	-1 -1 -5 686.674 136.398 3
532	-1 1 -4 1131.92 181.072 3
533	-1 -1 -4 1071.09 187.267 3
534	1 -1 -4 935.292 184.429 3
535	1 1 -4 930.370 167.740 3
536	1 -1 -3 786.644 293.820 2
537	-1 -1 -3 257.497 241.656 2
538	1 -1 -2 3939.65 449.759 2
539	-1 -1 -2 4463.63 494.275 2
540	-1 1 -2 4142.02 456.994 2
541	1 -1 -1 2389.19 275.913 2
542	1 1 0 13978.2 282.837 7
543	1 -2 -5 3339.33 245.721 3
544	-1 -2 -5 3068.62 222.658 3
545	1 2 -4 2473.95 239.956 3
546	-1 -2 -4 2196.17 235.741 3
547	1 -2 -4 2420.55 254.267 3
548	-1 -2 -4 3133.69 635.131 2
549	1 -2 -4 2848.90 593.567 2
550	-1 -2 -3 5213.27 666.001 2
551	1 -2 -3 4947.42 659.513 2
552	1 -2 -2 17458.5 929.449 2
553	-1 -2 -2 18405.6 1001.79 2
554	1 2 0 2262.54 165.818 7
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556	-1 -3 -5 913.790 140.772 3
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558	1 -3 -4 1449.41 208.975 3
559	-1 -3 -4 1502.40 201.077 3
560	-1 -3 -3 2257.86 501.138 2
561	1 -3 -3 2176.65 485.261 2
562	1 -3 -2 533.601 285.342 2
563	-1 -3 -2 529.016 303.674 2
564	-1 -3 -1 85182.3 1559.30 1
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567	-1 -4 -5 2353.51 178.337 3
568	1 -4 -5 2282.79 188.808 3
569	1 -4 -4 7159.78 395.656 3
570	-1 -4 -4 7306.29 380.642 3
571	1 -4 -3 267.152 253.938 2
572	-1 -4 -3 373.178 276.913 2
573	1 -4 -2 23879.0 1260.36 2
574	-1 -4 -1 15967.6 827.003 1
575	1 -4 -1 16330.8 782.092 1
576	-1 4 0 9908.20 322.146 7
577	1 4 0 11104.3 404.478 7
578	-1 4 3 205.638 135.269 5
579	1 4 3 353.507 173.368 5
580	1 -5 -5 74.2448 77.5880 3
581	-1 -5 -5-2.53471 51.9262 3
582	-1 -5 -4 1355.94 190.164 3
583	1 -5 -4 1311.52 201.441 3
584	1 -5 -3 6857.14 851.608 2
585	-1 -5 -3 8229.30 937.148 2
586	1 -5 -2 1274.29 385.808 2
587	1 -5 -1 3863.47 484.535 1
588	1 5 -1 4618.02 375.418 7
589	-1 -5 -1 3767.14 481.190 1
590	-1 5 3 8222.27 394.460 5
591	1 5 3 7785.22 395.550 5
592	1 -6 -4 97.8484 140.713 3
593	-1 -6 -4 50.1323 132.232 3
594	1 -6 -2 2795.54 258.386 4
595	-1 -6 -2 2513.72 247.557 4
596	1 -6 -1 9731.52 756.046 1
597	-1 -6 -1 9606.40 788.919 1
598	-1 -6 0-36.2820 201.680 1
599	1 -6 0-21.2166 197.403 1
600	1 6 2 2394.81 239.523 5
601	-1 6 2 2616.03 240.121 5
602	1 6 3 6116.83 367.754 5
603	-1 6 3 6182.18 369.791 5
604	1 -7 -4 213.150 116.572 3
605	-1 -7 -4 177.964 118.514 3
606	-1 -7 -2 2340.28 249.579 4
607	1 -7 -2 1557.56 406.849 2
608	1 -7 -2 2010.68 244.668 4
609	-1 -7 -1 3482.47 536.823 1
610	1 -7 0 4579.20 558.197 1
611	-1 7 0 5306.56 284.733 5
612	-1 -7 0 5250.73 627.983 1
613	1 7 1 4168.73 275.096 5
614	-1 7 1 4204.68 276.547 5
615	1 7 2 1924.61 242.037 5
616	-1 7 2 2098.67 236.561 5
617	-1 7 3 265.317 150.205 5
618	1 7 3 493.882 187.017 5
619	-1 -8 -4 99.5950 73.7294 3
620	1 -8 -4 316.663 87.7427 3
621	-1 -8 -2 2060.96 246.093 4
622	1 -8 -2 2231.61 250.405 4
623	1 -8 -1 518.912 165.823 4
624	-1 -8 -1 480.856 168.015 4
625	1 -8 0 6801.81 739.758 1
626	-1 8 0 7466.25 342.328 5
627	-1 -8 0 6544.46 781.147 1
628	1 -8 1 102.562 243.789 1
629	-1 -8 1 743.462 263.443 1
630	-1 8 1 278.611 167.446 5
631	1 8 1 463.243 154.051 5
632	1 8 2 2151.94 251.960 5
633	-1 8 2 2601.30 264.926 5
634	-1 8 3 1467.54 204.170 5
635	1 8 3 1519.96 207.815 5
636	-1 -9 -2 494.295 166.421 4
637	1 -9 -2 410.383 165.052 4
638	1 -9 -1 1453.04 215.326 4
639	-1 -9 -1 1781.72 233.533 4
640	-1 9 0 174.240 133.136 5
641	1 9 1 1753.61 209.745 5
642	-1 9 1 1717.84 210.952 5
643	-1 9 2 421.576 166.104 5
644	1 9 2 546.143 167.968 5
645	-1 9 3-74.7848 112.841 5
646	1 9 3 178.506 115.407 5
647	-1 -10 -1 1999.39 221.958 4
648	1 -10 -1 2120.35 231.150 4
649	-1 10 1 2290.86 227.357 5
650	1 10 1 2073.51 208.907 5
651	-1 10 2 197.584 122.933 5
652	1 10 2 202.972 122.709 5
653	-1 -11 -1 88.0831 104.600 4
654	1 -11 -1 27.2996 98.4443 4
655	-1 -11 0 680.514 136.025 4
656	1 -11 0 739.225 141.404 4
657	1 11 1 53.1970 91.7518 5
658	-1 11 1-63.6878 94.2621 5
659	-1 11 2 614.457 103.135 5
660	-1 -12 0 305.181 74.2036 4
661	1 -12 0 310.320 78.6373 4
662	2 0 -5 3810.52 278.390 3
663	-2 0 -4 7631.41 389.948 3
664	2 0 -4 7250.93 410.515 3
665	2 0 -3 1724.55 424.353 2
666	-2 0 -3 1605.48 403.085 2
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668	2 0 -2 68395.7 1646.70 2
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671	2 0 0 3232.06 130.946 7
672	2 -1 -5 11559.8 450.132 3
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678	2 -1 -3 3169.57 530.441 2
679	-2 -1 -3 3467.71 544.778 2
680	-2 -1 -2 8800.31 660.527 2
681	2 -1 -2 9563.73 653.314 2
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685	2 -2 -5 428.409 131.058 3
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705	-2 -3 -2 297.784 272.969 2
706	-2 -3 -1 1553.17 279.136 1
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708	2 3 3 12087.0 429.134 5
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710	2 -4 -4 2338.03 249.740 3
711	-2 -4 -4 1905.87 218.176 3
712	-2 -4 -3 3818.36 603.741 2
713	2 -4 -3 3645.66 616.959 2
714	2 -4 -2 4026.52 558.131 2
715	2 -4 -1 36806.3 1144.48 1
716	-2 -4 -1 38379.7 1275.29 1
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720	2 -5 -5 91.1080 80.3085 3
721	2 -5 -4 490.671 155.829 3
722	-2 -5 -4 90.1531 104.369 3
723	2 -5 -3 6172.52 792.113 2
724	-2 -5 -3 5577.54 808.333 2
725	2 -5 -2 534.788 338.443 2
726	2 5 -1 14921.4 682.917 7
727	2 -5 -1 15790.5 865.811 1
728	-2 -5 -1 15160.8 895.713 1
729	2 -5 0 1923.58 296.628 1
730	2 5 0 2329.33 247.744 7
731	-2 5 3 6521.33 351.112 5
732	2 5 3 7868.34 396.297 5
733	2 -6 -5 762.115 95.8738 3
734	2 -6 -4 57.7847 128.826 3
735	-2 -6 -4 67.5714 102.513 3
736	-2 -6 -2 2192.68 238.529 4
737	2 -6 -2 1912.93 479.174 2
738	2 -6 -2 2380.57 248.726 4
739	-2 -6 -1 1637.17 378.570 1
740	2 -6 -1 1269.68 334.448 1
741	2 -6 0 2214.73 354.094 1
742	-2 -6 0 1988.16 366.591 1
743	-2 6 2 2194.73 224.396 5
744	2 6 2 1994.76 233.242 5
745	2 6 3 981.640 207.231 5
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747	-2 -7 -4 197.979 103.905 3
748	2 -7 -4-23.2687 99.7102 3
749	2 -7 -2 1249.06 432.625 2
750	-2 -7 -2 1768.92 225.628 4
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763	2 -8 -4 124.860 84.8925 3
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767	-2 -8 -1 2986.75 276.484 4
768	-2 8 0 790.836 169.417 5
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770	2 -8 1 2996.52 513.749 1
771	2 8 1 2891.90 257.577 5
772	-2 8 1 2549.25 253.380 5
773	-2 -8 1 2362.34 465.851 1
774	2 8 2 485.729 179.547 5
775	-2 8 2 710.248 183.704 5
776	2 8 3 2921.35 250.349 5
777	-2 8 3 2732.86 244.618 5
778	2 -9 -2 2498.41 257.659 4
779	-2 -9 -2 2463.72 247.847 4
780	-2 -9 -1 677.801 168.437 4
781	2 -9 -1 535.852 169.990 4
782	-2 9 0 444.415 152.101 5
783	2 9 1 448.144 163.137 5
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785	2 9 2 2557.48 241.737 5
786	-2 9 2 2568.02 255.126 5
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788	2 -10 -1 782.721 166.144 4
789	-2 -10 -1 874.860 173.133 4
790	2 -10 0 56.5452 134.567 4
791	-2 10 0 104.493 112.903 5
792	-2 10 1 755.345 153.722 5
793	2 10 1 901.860 163.444 5
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796	-2 -11 -1 337.402 113.645 4
797	2 -11 -1 363.833 119.658 4
798	-2 -11 0 84.8488 95.2967 4
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800	-2 11 1 298.233 111.285 5
801	2 -11 1 349.039 121.874 4
802	-2 11 2 607.707 106.745 5
803	-2 -12 0 120.927 63.1439 4
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808	-3 0 -3 496.523 285.365 2
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812	-3 0 -1 44.4133 142.807 2
813	3 0 0 9.95340 77.3456 7
814	3 -1 -5 1307.81 180.015 3
815	3 -1 -4 7245.67 420.435 3
816	-3 1 -4 6931.50 352.359 3
817	3 1 -4 6951.87 404.539 3
818	-3 -1 -4 7113.65 378.949 3
819	3 -1 -3 12187.1 961.682 2
820	-3 -1 -3 12193.5 976.771 2
821	3 -1 -2 5915.12 522.850 2
822	-3 1 -2 5904.04 510.659 2
823	-3 -1 -2 6413.31 566.538 2
824	3 -1 -1 26969.9 742.558 2
825	3 -1 0 661.842 89.8645 7
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829	3 2 -4 285.821 144.495 3
830	-3 -2 -4 236.624 126.563 3
831	3 -2 -4 210.951 138.101 3
832	3 -2 -3 3118.57 532.798 2
833	3 2 -3 3269.56 244.300 3
834	-3 -2 -3 2740.25 522.120 2
835	-3 -2 -2 353.952 259.743 2
836	3 -2 -2 193.995 209.266 2
837	3 2 0 105558. 1193.74 7
838	3 -3 -5 422.688 121.621 3
839	-3 -3 -4 1430.93 192.001 3
840	3 -3 -4 1074.50 197.503 3
841	3 -3 -3 5074.11 675.208 2
842	-3 -3 -3 4718.96 653.429 2
843	3 3 -3 5017.14 306.378 3
844	3 -3 -2 8.94686 189.552 2
845	-3 -3 -2 136.159 213.877 2
846	-3 -3 -1 2652.53 347.774 1
847	3 3 0 26490.9 667.102 7
848	3 3 3 4736.55 290.389 5
849	3 -4 -5 311.415 112.263 3
850	3 -4 -4 794.089 180.146 3
851	-3 -4 -4 349.726 133.652 3
852	-3 -4 -3 1873.84 482.804 2
853	3 -4 -3 1381.83 409.440 2
854	3 -4 -2 3004.50 484.940 2
855	-3 -4 -1 2871.61 459.173 1
856	3 4 0 10070.6 454.144 7
857	-3 4 3 1498.50 193.290 5
858	3 4 3 1875.21 222.724 5
859	3 -5 -5 159.835 86.5455 3
860	-3 -5 -4 362.129 124.326 3
861	3 -5 -4 661.209 177.303 3
862	3 -5 -3 1666.43 468.547 2
863	-3 -5 -3 2878.61 565.093 2
864	3 -5 -2 8673.01 819.212 2
865	3 -5 -2 9582.23 418.876 4
866	3 5 -1 490.824 184.458 7
867	-3 -5 -1 373.424 283.215 1
868	3 5 0 2812.11 286.959 7
869	3 -5 0 1154.15 248.318 1
870	3 5 2 9162.72 395.163 5
871	3 5 3 3170.51 270.957 5
872	-3 5 3 2627.31 247.711 5
873	3 -6 -5 1193.50 111.797 3
874	-3 -6 -4 2192.28 205.633 3
875	3 -6 -4 2192.44 243.329 3
876	3 -6 -2 3123.83 272.891 4
877	-3 -6 -2 2755.49 258.280 4
878	-3 -6 -1 6436.02 666.682 1
879	-3 -6 0-19.5023 175.643 1
880	3 -6 0 33.0254 184.805 1
881	3 6 2 3175.11 273.754 5
882	-3 6 2 2846.49 248.992 5
883	3 6 3 4937.82 334.170 5
884	-3 6 3 4431.25 306.474 5
885	3 -7 -4 111.876 117.322 3
886	-3 -7 -4-30.0108 81.1996 3
887	-3 -7 -2 94.9683 140.788 4
888	3 -7 -2 62.9017 149.294 4
889	3 -7 -1 3900.71 292.940 4
890	-3 -7 -1 3354.65 541.528 1
891	-3 7 0 4140.52 275.454 5
892	3 -7 0 3782.75 501.098 1
893	-3 -7 0 4258.18 578.995 1
894	3 7 1 3553.02 253.880 5
895	-3 7 1 3448.49 269.962 5
896	-3 7 2 180.659 146.001 5
897	3 7 2 185.533 161.653 5
898	-3 7 3 2112.21 232.133 5
899	3 7 3 2090.26 243.230 5
900	3 -8 -4 342.886 97.5083 3
901	-3 -8 -2 643.177 167.024 4
902	3 -8 -2 492.227 180.458 4
903	3 -8 -1 2656.75 264.295 4
904	-3 -8 -1 2755.92 262.006 4
905	-3 8 0-24.8452 138.033 5
906	3 -8 0-376.655 274.482 1
907	-3 8 1 2930.82 258.501 5
908	-3 -8 1 2992.79 548.349 1
909	3 8 1 2622.93 260.497 5
910	3 8 2 567.325 181.568 5
911	-3 8 2 541.843 177.307 5
912	3 8 3 80.0821 127.509 5
913	-3 8 3 307.307 143.308 5
914	-3 -9 -2 457.255 147.442 4
915	3 -9 -2 430.106 154.682 4
916	3 -9 -1 1917.17 247.643 4
917	-3 -9 -1 2289.61 254.030 4
918	-3 9 0 1678.92 203.127 5
919	3 9 1 1874.75 210.396 5
920	-3 9 1 2005.64 228.950 5
921	3 9 2 753.064 164.664 5
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924	3 -10 -1 126.030 117.668 4
925	-3 -10 -1 289.447 134.552 4
926	3 -10 0 20.4657 122.544 4
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928	3 10 1 185.166 115.650 5
929	-3 10 1 62.8865 126.169 5
930	3 10 2 333.717 125.396 5
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932	-3 10 3 683.124 106.521 5
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934	-3 -11 -1 1188.19 154.629 4
935	3 -11 0 229.465 114.376 4
936	-3 -11 0 162.144 95.5178 4
937	-3 11 1 1351.38 149.941 5
938	3 -11 1 1249.84 165.084 4
939	-3 11 2 254.408 88.3570 5
940	3 -11 2 156.866 74.2736 4
941	3 -12 0 39.5779 65.6175 4
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952	4 -1 -4 4076.78 329.007 3
953	4 -1 -3 319.482 283.328 2
954	-4 -1 -3 289.461 267.681 2
955	-4 1 -2 5574.57 482.351 2
956	4 -1 -2 4642.93 473.764 2
957	-4 -1 -2 5194.86 521.878 2
958	4 -1 -1 1066.34 193.278 2
959	4 1 0 364.668 162.071 7
960	4 -1 0 199.090 90.5622 7
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963	4 2 -4 885.503 174.274 3
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966	-4 -2 -3 1982.79 429.070 2
967	-4 -2 -2 1638.66 379.809 2
968	4 -2 -2 623.694 250.083 2
969	4 -2 -1 37372.0 990.164 2
970	4 -2 0 15124.2 385.057 1
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978	4 -3 -2 22315.1 1110.17 2
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980	4 3 0 6277.56 373.189 7
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987	-4 -4 -1 8232.90 651.408 1
988	4 4 -1 7765.51 515.771 7
989	4 4 0 12906.4 550.822 7
990	4 -4 0 12183.3 578.798 1
991	4 4 3 3067.20 260.916 5
992	-4 4 3 2359.46 212.225 5
993	4 -5 -5 92.5117 77.8473 3
994	4 -5 -4 272.595 152.905 3
995	-4 -5 -3 9754.69 1026.00 2
996	4 -5 -3 10864.7 1003.31 2
997	4 -5 -2 1700.07 203.994 4
998	4 -5 -2 1522.52 388.832 2
999	4 5 -1 18115.8 814.660 7
1000	-4 -5 -1 19154.1 1062.14 1
1001	4 -5 0 1159.96 266.474 1
1002	4 5 0 1543.42 242.632 7
1003	-4 5 2 1536.42 182.415 5
1004	4 5 2 1563.28 201.005 5
1005	4 5 3 10173.9 439.913 5
1006	-4 5 3 9958.13 410.952 5
1007	4 -6 -5 16.8821 51.9292 3
1008	4 -6 -4 59.9117 118.596 3
1009	-4 -6 -2-9.96033 125.133 4
1010	4 -6 -2 103.773 134.119 4
1011	4 6 -1 777.075 230.918 7
1012	-4 -6 -1 851.838 303.492 1
1013	-4 -6 0 1067.47 294.710 1
1014	4 -6 0 782.910 245.075 1
1015	-4 6 1 726.498 155.036 5
1016	4 6 2 32.0869 164.880 5
1017	-4 6 2-109.763 123.419 5
1018	4 6 3 3.09907 143.169 5
1019	-4 6 3 140.138 138.209 5
1020	4 -7 -4 355.732 124.128 3
1021	4 -7 -2 957.203 190.451 4
1022	-4 -7 -2 699.454 161.494 4
1023	4 -7 -1 1783.65 225.661 4
1024	-4 -7 -1 1333.12 351.198 1
1025	-4 7 0 1233.87 193.267 5
1026	4 -7 0 411.327 265.427 1
1027	-4 -7 0 930.096 359.921 1
1028	-4 7 1 1955.80 240.247 5
1029	4 7 1 1487.17 214.510 5
1030	-4 7 2 818.166 177.470 5
1031	4 7 2 882.653 206.052 5
1032	4 7 3 237.977 159.935 5
1033	-4 7 3 62.9919 144.668 5
1034	4 -8 -4 95.1707 72.9330 3
1035	4 -8 -2-15.2575 129.703 4
1036	-4 -8 -2 37.1061 128.149 4
1037	-4 -8 -1 871.136 174.754 4
1038	4 -8 -1 918.723 182.785 4
1039	-4 -8 0 5513.39 771.857 1
1040	-4 8 0 5425.69 327.404 5
1041	-4 -8 1 1280.30 384.342 1
1042	4 8 1 1130.57 191.818 5
1043	-4 8 1 791.600 182.914 5
1044	4 8 2 93.6608 154.713 5
1045	-4 8 2 127.434 143.232 5
1046	-4 8 3 524.734 158.312 5
1047	-4 -9 -2 1016.06 165.151 4
1048	4 -9 -1 380.511 152.820 4
1049	-4 -9 -1 419.075 157.412 4
1050	-4 9 0 73.2111 123.534 5
1051	-4 9 1 533.201 167.685 5
1052	4 9 1 253.900 140.215 5
1053	4 9 2 964.326 171.014 5
1054	-4 9 2 1516.02 209.980 5
1055	-4 9 3 133.121 114.063 5
1056	4 -10 -1 43.0482 128.926 4
1057	-4 -10 -1 50.6481 116.434 4
1058	4 -10 0 147.643 135.047 4
1059	-4 10 0 112.299 128.939 5
1060	4 10 1 60.3720 105.205 5
1061	-4 10 1 106.445 124.832 5
1062	-4 10 2 167.099 128.684 5
1063	-4 10 3-19.3417 77.4290 5
1064	-4 -11 -1 682.550 119.023 4
1065	4 -11 -1 851.762 138.032 4
1066	4 -11 0-65.2548 102.797 4
1067	-4 -11 0-8.99863 91.3758 4
1068	4 -11 1 827.488 143.014 4
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1070	4 -11 2 29.8768 60.9330 4
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1075	-5 0 -2-2.04318 166.558 2
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1078	5 -1 -5 4393.12 290.927 3
1079	5 -1 -4 569.362 170.733 3
1080	5 1 -4 885.320 184.621 3
1081	5 -1 -3 7359.60 779.770 2
1082	-5 -1 -3 7114.65 755.638 2
1083	5 -1 -3 6614.28 355.410 3
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1090	5 -1 0 43303.8 632.147 7
1091	5 -2 -5 588.671 145.365 3
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1094	5 -2 -3 3431.52 548.847 2
1095	-5 -2 -3 3138.62 546.974 2
1096	5 2 -3 3397.63 258.627 3
1097	5 -2 -2 1516.89 329.553 2
1098	-5 -2 -2 1375.10 337.789 2
1099	5 -2 -1 33096.5 905.429 2
1100	5 -2 0 1097.36 124.739 1
1101	5 2 0 1067.20 204.278 7
1102	5 -3 -5 473.281 133.363 3
1103	5 -3 -4 346.895 158.032 3
1104	5 -3 -3 3297.40 565.360 2
1105	-5 -3 -3 2534.13 515.251 2
1106	5 3 -3 2827.13 250.831 3
1107	-5 -3 -2 3019.30 468.647 2
1108	5 -3 -2 2739.04 433.143 2
1109	-5 -3 -1 23524.4 872.406 1
1110	5 -3 0 35401.4 759.250 1
1111	5 3 0 32954.1 860.616 7
1112	5 -4 -5 14.8389 88.7471 3
1113	5 -4 -4 400.004 160.912 3
1114	-5 -4 -3 474.267 306.629 2
1115	5 -4 -3 554.165 287.154 2
1116	5 -4 -2 3888.77 509.609 2
1117	5 4 -1 41.5119 171.835 7
1118	-5 -4 -1 370.654 268.235 1
1119	5 -4 0 1603.46 242.949 1
1120	5 4 0 2026.72 261.477 7
1121	5 -5 -5 193.706 86.7134 3
1122	5 -5 -4 382.521 164.639 3
1123	-5 -5 -3 1290.66 394.550 2
1124	5 -5 -3 896.988 300.492 2
1125	5 -5 -2 4460.82 303.930 4
1126	5 5 -2 4539.78 501.965 7
1127	5 -5 -2 3384.70 511.801 2
1128	5 5 -1 4326.02 442.782 7
1129	-5 -5 -1 5242.40 573.588 1
1130	5 -5 0 8084.65 554.811 1
1131	5 5 0 8537.56 515.656 7
1132	5 5 2 4274.14 301.800 5
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1142	5 6 -1 6326.36 529.998 7
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1154	5 -7 -1 1851.97 223.825 4
1155	-5 -7 -1 1903.90 430.602 1
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1177	-5 9 0 703.408 168.100 5
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1190	-5 -11 -1-43.3470 81.5753 4
1191	5 -11 0-16.6719 91.3617 4
1192	-5 -11 0-104.524 87.8752 4
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1207	6 1 -3 7530.32 371.947 3
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1222	6 -2 -2 53.0732 199.718 2
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1227	-6 -3 -3 1541.87 395.460 2
1228	6 3 -3 1466.47 187.492 3
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1231	6 3 -1 11856.3 634.636 7
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1246	6 -5 -4 3598.99 303.321 3
1247	-6 -5 -3 855.091 380.537 2
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1252	-6 -5 -1 1126.94 348.640 1
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1255	6 -5 0 5568.40 468.610 1
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1300	6 -9 0 1992.40 233.552 4
1301	-6 9 0 2179.99 228.110 5
1302	6 9 1 1796.55 200.513 5
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1334	-7 -1 -2 4305.23 458.943 2
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1348	7 -2 -1 12939.0 499.677 7
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1350	7 -3 -5 1207.97 162.818 3
1351	7 -3 -4 6343.43 391.248 3
1352	-7 -3 -3 1326.70 410.411 2
1353	7 -3 -3 1114.29 302.441 2
1354	7 -3 -2 7346.82 604.936 2
1355	-7 -3 -2 7209.81 704.253 2
1356	7 3 -1 1017.14 243.882 7
1357	7 -3 -1 691.290 186.248 2
1358	-7 -3 -1 691.995 239.625 1
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1362	-7 -4 -3 610.122 280.389 2
1363	7 -4 -3 253.059 204.150 2
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1365	7 4 -1 695.463 238.294 7
1366	7 -4 -1 437.287 179.680 2
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1369	7 -5 -5 90.1974 67.2133 3
1370	7 -5 -4 780.295 172.265 3
1371	7 5 -3 199.704 213.319 7
1372	-7 -5 -3 854.877 325.592 2
1373	7 5 -2 3266.47 476.353 7
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1471	-8 -3 -3 1632.20 420.345 2
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1500	-8 6 0 547.932 139.962 5
1501	-8 -6 0 13.9736 206.917 1
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1508	8 -7 -1 827.719 191.467 4
1509	-8 7 -1 908.251 172.477 5
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1512	-8 7 1 584.558 178.615 5
1513	8 7 1 513.797 165.693 5
1514	-8 7 2 1767.62 218.901 5
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1516	8 -8 -4 1070.78 104.544 3
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1518	-8 8 -1 3290.67 259.176 5
1519	-8 8 0 996.415 189.860 5
1520	8 -8 0 1172.80 192.028 4
1521	-8 8 1 3730.96 295.993 5
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1606	-9 -6 -1 4431.56 607.499 1
1607	-9 -6 0 4204.35 538.051 1
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1609	9 6 0 4144.87 495.383 7
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1703	-10 -6 0 148.466 208.284 1
1704	-10 6 1 1691.00 218.955 5
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1723	-10 9 -1 1656.42 190.975 5
1724	-10 9 0 78.7348 116.928 5
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1727	-10 9 2 612.189 131.633 5
1728	-10 9 3 296.210 85.4665 5
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1767	11 3 -2 344.396 237.650 7
1768	11 3 -1 5317.91 550.388 7
1769	-11 -3 0 2620.54 313.611 1
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1773	11 -4 -4 1102.31 176.829 3
1774	11 -4 -3 693.138 165.104 3
1775	11 4 -2 1510.99 380.022 7
1776	-11 -4 -2 1109.95 350.136 2
1777	11 4 -1 4790.55 549.682 7
1778	-11 -4 0 4552.22 470.167 1
1779	11 4 0 4957.42 530.167 7
1780	-11 4 1 5166.66 272.679 5
1781	11 4 2 2151.82 224.894 6
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1783	11 4 4 1018.63 157.765 6
1784	11 -5 -4 330.084 117.798 3
1785	11 5 -2 142.924 216.664 7
1786	-11 -5 -2 411.765 264.750 2
1787	11 5 -1 4945.67 581.741 7
1788	-11 -5 0 409.622 217.512 1
1789	11 5 0 396.672 252.625 7
1790	-11 5 1 4714.63 290.943 5
1791	-11 5 2 370.752 154.624 5
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1794	11 5 4 424.871 106.663 6
1795	11 -6 -4 1728.97 171.546 3
1796	11 6 -1 1108.09 358.180 7
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1798	11 6 0 1799.54 390.409 7
1799	-11 -6 0 1852.34 406.107 1
1800	-11 6 1 790.824 176.643 5
1801	-11 6 2 3732.97 276.418 5
1802	-11 6 3 267.036 124.745 5
1803	11 -7 -4 148.752 68.8798 3
1804	-11 7 -2 411.449 129.565 5
1805	-11 7 -1 823.712 168.147 5
1806	11 -7 -1 862.191 177.129 4
1807	-11 7 0 1551.65 196.979 5
1808	-11 7 1 1087.50 198.556 5
1809	-11 7 2 524.017 160.628 5
1810	-11 7 3 982.544 147.174 5
1811	11 -8 -3 313.194 109.655 3
1812	-11 8 -1 2510.26 232.793 5
1813	-11 8 0 191.520 140.582 5
1814	-11 8 1 2483.31 236.049 5
1815	-11 8 2 651.693 147.646 5
1816	-11 8 3 341.802 110.741 5
1817	-11 9 -1 138.904 122.374 5
1818	-11 9 0 1047.80 164.847 5
1819	-11 9 1 57.6144 108.484 5
1820	-11 9 2 71.1954 94.9811 5
1821	-11 10 0 89.9282 95.4315 5
1822	-11 10 1 3006.76 180.331 5
1823	-11 10 2 316.677 84.0309 5
1824	12 0 -4 348.352 133.905 3
1825	12 0 -3 3719.98 558.093 7
1826	12 0 -3 3822.03 285.411 3
1827	12 0 -2 13581.1 925.255 7
1828	12 0 -1 8302.23 615.897 7
1829	12 0 0 4242.66 428.495 7
1830	12 0 2 14109.3 486.161 6
1831	12 0 5 2176.43 160.303 6
1832	12 1 -4 350.262 136.388 3
1833	12 -1 -4 214.266 127.117 3
1834	12 -1 -3 801.103 163.010 3
1835	12 1 -3 1017.03 173.005 3
1836	12 -1 -2 1946.47 394.536 7
1837	12 1 -2 2682.23 468.263 7
1838	12 -1 -1 6317.30 518.538 7
1839	12 1 -1 5783.54 542.058 7
1840	12 -1 0 14689.2 709.350 7
1841	12 1 0 14398.2 775.520 7
1842	12 -1 2 2551.86 227.676 6
1843	12 -1 4 338.512 147.394 6
1844	12 -1 5 385.439 87.0571 6
1845	12 1 5 315.604 97.9128 6
1846	12 -2 -4 371.925 138.584 3
1847	12 2 -3 918.425 285.115 7
1848	12 -2 -3 1164.57 190.619 3
1849	12 2 -2 1713.01 413.912 7
1850	12 2 -1 6675.60 603.885 7
1851	12 2 0 5812.87 538.760 7
1852	12 2 2 2525.70 229.708 6
1853	12 -2 2 2095.86 204.345 6
1854	12 -2 3 971.230 173.214 6
1855	12 -2 4 208.446 113.632 6
1856	12 2 5 205.567 80.3950 6
1857	12 -3 -5 294.398 68.7653 3
1858	12 -3 -4 1223.39 175.577 3
1859	12 -3 -3 278.096 131.770 3
1860	12 3 -2 1505.46 368.624 7
1861	12 3 -1 1654.35 374.118 7
1862	12 3 0 555.785 278.877 7
1863	12 3 2 1214.62 181.534 6
1864	12 3 4 1108.24 176.860 6
1865	12 3 5 247.010 67.5368 6
1866	12 -4 -4 2435.29 214.688 3
1867	12 -4 -3 468.087 151.610 3
1868	12 4 -2 1133.94 319.424 7
1869	12 4 -1 4258.53 529.421 7
1870	-12 -4 0 1980.24 319.243 1
1871	12 4 0 3066.26 465.442 7
1872	12 4 1 4800.17 283.320 6
1873	-12 4 1 5004.09 281.187 5
1874	-12 4 2 338.504 141.967 5
1875	12 4 2 231.217 119.946 6
1876	12 4 3 918.146 158.676 6
1877	12 4 4 2532.70 207.245 6
1878	12 -5 -4 3603.52 237.889 3
1879	12 -5 -3 131.572 115.777 3
1880	12 5 -2 7663.10 719.769 7
1881	12 5 -1 554.262 283.414 7
1882	-12 -5 0 236.095 150.949 1
1883	12 5 0 96.9935 260.846 7
1884	-12 5 1 382.465 150.803 5
1885	12 5 2 8095.82 375.823 6
1886	-12 5 2 7284.72 362.919 5
1887	12 5 3 227.289 122.634 6
1888	12 5 4 3568.54 207.714 6
1889	12 -6 -4 682.566 113.411 3
1890	12 -6 -3 168.517 107.598 3
1891	12 6 -1 2559.27 502.612 7
1892	-12 6 0 83.1376 123.589 5
1893	12 6 0-840.912 343.014 7
1894	-12 -6 0-583.333 262.866 1
1895	-12 6 1 1942.49 223.241 5
1896	-12 -6 1 2042.29 361.520 1
1897	-12 6 2 842.360 179.992 5
1898	12 -7 -3 600.584 126.750 3
1899	-12 7 -2 998.184 168.932 5
1900	-12 7 -1 758.269 154.407 5
1901	-12 7 0 875.492 171.231 5
1902	-12 7 1 854.602 176.557 5
1903	-12 7 2 849.020 160.361 5
1904	-12 7 3 519.775 121.844 5
1905	12 -8 -3 314.023 92.7549 3
1906	-12 8 -1 592.745 149.568 5
1907	-12 8 0 228.314 132.316 5
1908	-12 8 1 543.761 149.336 5
1909	-12 8 2 2194.48 198.447 5
1910	-12 8 3 542.774 105.651 5
1911	-12 9 -1 457.670 121.282 5
1912	-12 9 0 1044.46 155.197 5
1913	-12 9 1 272.165 110.764 5
1914	-12 9 2 171.662 100.796 5
1915	-12 10 0 134.024 85.7548 5
1916	-12 10 1 35.7746 78.3558 5
1917	-12 10 2 170.719 60.9139 5
1918	13 0 -4-110.726 120.986 3
1919	13 0 -3-86.9456 104.817 3
1920	13 0 -2-463.905 216.096 7
1921	13 0 -1 83.2105 166.423 7
1922	13 0 0-168.697 200.374 7
1923	13 0 2 93.4141 119.228 6
1924	13 0 3 28.1321 141.011 6
1925	13 0 4-95.5933 131.186 6
1926	13 0 5-117.960 67.5729 6
1927	13 -1 -4 332.052 122.721 3
1928	13 1 -3 6669.29 351.899 3
1929	13 -1 -3 6513.34 362.203 3
1930	13 1 -2 1946.63 389.053 7
1931	13 -1 -1 53.4283 166.910 7
1932	13 1 -1 211.292 218.970 7
1933	13 -1 0 40169.9 1255.61 7
1934	13 1 0 38161.0 1331.50 7
1935	13 -1 2 2124.65 219.587 6
1936	13 1 2 2365.00 225.196 6
1937	13 -1 3 6085.73 364.744 6
1938	13 1 3 6429.98 384.560 6
1939	13 -1 4 254.971 134.461 6
1940	13 1 4 279.463 144.828 6
1941	13 1 5 84.7366 67.8721 6
1942	13 -2 -4 432.481 130.717 3
1943	13 -2 -3 2295.11 237.808 3
1944	13 2 -2 1026.09 325.778 7
1945	13 2 -1 1689.46 371.843 7
1946	13 2 0 12918.3 827.486 7
1947	13 -2 2 1486.81 186.906 6
1948	13 2 2 1393.68 191.277 6
1949	13 -2 3 2595.99 239.366 6
1950	13 2 3 2668.48 259.561 6
1951	13 -2 4 624.848 145.286 6
1952	13 2 4 601.882 149.863 6
1953	13 2 5 132.161 65.8948 6
1954	13 -3 -4 3870.27 259.558 3
1955	13 -3 -3 950.347 167.557 3
1956	13 3 -2 1040.56 309.345 7
1957	13 -3 -1 12702.2 506.997 6
1958	13 3 -1 12377.9 486.942 6
1959	13 3 -1 13705.1 932.399 7
1960	13 3 0 14.3028 148.277 7
1961	13 3 1 13511.0 458.785 6
1962	13 3 2 1564.01 194.779 6
1963	13 3 3 891.991 183.722 6
1964	13 3 4 3881.19 267.554 6
1965	13 -4 -4 526.501 123.485 3
1966	13 -4 -3 1417.30 191.867 3
1967	13 4 -2 2477.29 495.778 7
1968	13 4 -1 1497.56 407.536 7
1969	13 4 0 743.060 251.962 7
1970	-13 4 1 1145.60 166.788 5
1971	13 4 1 882.153 156.914 6
1972	13 4 2 3745.93 278.820 6
1973	13 4 3 1577.32 199.770 6
1974	13 4 4 640.860 128.232 6
1975	13 -5 -4 228.099 92.1206 3
1976	13 -5 -3 80.4730 112.202 3
1977	13 5 -1 2099.12 420.644 7
1978	13 5 0 668.172 262.551 7
1979	-13 5 1 1740.95 212.653 5
1980	13 5 2 2915.17 246.572 6
1981	-13 5 2 3259.02 257.629 5
1982	13 5 3-64.8951 94.8488 6
1983	13 5 4 125.812 82.6179 6
1984	13 -6 -4 847.597 104.596 3
1985	13 -6 -3 1110.51 161.867 3
1986	-13 6 0 209.131 132.376 5
1987	13 6 0 694.371 306.314 7
1988	-13 6 1 655.423 170.156 5
1989	-13 6 2 723.152 156.177 5
1990	13 -7 -3 274.970 98.3159 3
1991	-13 7 -2 333.922 132.134 5
1992	-13 7 -1 1443.87 186.634 5
1993	-13 7 0 839.255 167.942 5
1994	-13 7 1 1534.64 207.158 5
1995	-13 7 2 82.8095 127.121 5
1996	-13 8 -1 187.421 122.169 5
1997	-13 8 0 4662.06 280.762 5
1998	-13 8 1 77.6778 120.585 5
1999	-13 8 2 32.0070 107.820 5
2000	-13 9 -1 1380.25 156.901 5
2001	-13 9 0 744.525 135.738 5
2002	-13 9 1 1018.14 135.225 5
2003	-13 9 2 1090.54 128.264 5
2004	-13 10 0 2398.90 160.056 5
2005	-13 10 1 464.013 90.0860 5
2006	14 0 -2 5983.63 651.991 7
2007	14 0 -1 4631.82 327.717 6
2008	14 0 -1 4662.22 530.838 7
2009	14 0 0 4594.32 504.641 7
2010	14 0 1 5318.77 317.181 6
2011	14 0 2 5558.55 338.380 6
2012	14 0 3 1997.80 241.665 6
2013	14 0 4 1318.56 193.634 6
2014	14 -1 -4 3739.90 250.076 3
2015	14 -1 -3 1671.42 193.997 3
2016	14 1 -2 5065.18 632.548 7
2017	14 1 -1 747.322 272.736 7
2018	14 -1 -1 866.808 196.342 6
2019	14 1 -1 814.704 183.774 6
2020	14 -1 -1 665.428 239.273 7
2021	14 1 0 6071.03 599.207 7
2022	14 -1 1 841.220 168.091 6
2023	14 1 1 696.396 143.124 6
2024	14 1 2 4431.20 301.848 6
2025	14 -1 2 4416.78 299.560 6
2026	14 -1 3 1812.54 216.622 6
2027	14 1 3 1724.13 221.843 6
2028	14 -1 4 3352.68 256.683 6
2029	14 1 4 3542.33 275.658 6
2030	14 -2 -4 70.1801 94.2410 3
2031	14 -2 -3 381.500 127.780 3
2032	14 2 -2 329.005 215.663 7
2033	14 2 -1 2370.03 426.512 7
2034	14 -2 -1 2382.05 253.190 6
2035	14 2 -1 2254.52 244.044 6
2036	14 2 0 1691.99 196.744 6
2037	14 2 0 1165.57 308.916 7
2038	14 -2 1 2479.29 222.547 6
2039	14 2 1 2244.24 217.770 6
2040	14 -2 2 263.607 125.783 6
2041	14 2 2 165.260 128.411 6
2042	14 -2 3 442.884 135.912 6
2043	14 2 3 545.023 167.599 6
2044	14 -2 4-26.4961 94.0339 6
2045	14 2 4 3.15878 109.434 6
2046	14 -3 -4 304.568 106.804 3
2047	14 -3 -3 236.828 109.383 3
2048	14 3 -2 9189.15 823.164 7
2049	14 3 -1 2536.05 445.132 7
2050	14 -3 -1 2430.78 256.318 6
2051	14 3 -1 2639.33 264.506 6
2052	14 3 0 1502.56 194.072 6
2053	14 3 0 1128.63 301.082 7
2054	14 3 1 2450.90 229.553 6
2055	14 3 2 9576.26 428.516 6
2056	14 3 3 517.308 153.358 6
2057	14 3 4 71.3257 103.536 6
2058	14 -4 -4 104.097 82.3965 3
2059	14 -4 -3 471.496 134.281 3
2060	14 4 -1 322.337 245.937 7
2061	14 4 -1 32.7845 135.100 6
2062	14 4 0 826.960 161.329 6
2063	14 4 0 113.948 248.229 7
2064	-14 4 1 172.451 120.636 5
2065	14 4 1-34.8812 113.263 6
2066	14 4 2 99.4743 124.133 6
2067	14 4 3 444.850 126.005 6
2068	14 4 4 22.1009 82.0393 6
2069	14 -5 -4 1930.48 145.763 3
2070	14 -5 -3 509.494 120.395 3
2071	14 5 -1 2120.38 498.314 7
2072	14 5 0 4583.45 631.266 7
2073	-14 5 1 2206.40 226.101 5
2074	-14 5 2 290.471 143.878 5
2075	14 5 2 279.864 135.009 6
2076	14 5 3 488.652 129.344 6
2077	14 5 4 2415.10 155.334 6
2078	14 -6 -3 367.987 104.253 3
2079	-14 6 0 4107.86 267.981 5
2080	-14 6 1 193.201 157.591 5
2081	-14 6 2 433.917 142.401 5
2082	-14 7 -2 253.433 116.121 5
2083	-14 7 -1 846.406 167.236 5
2084	-14 7 0 5102.51 297.359 5
2085	-14 7 1 1012.78 179.246 5
2086	-14 7 2 217.364 112.188 5
2087	-14 8 -2 449.392 108.973 5
2088	-14 8 -1 1351.40 177.738 5
2089	-14 8 0 206.564 126.104 5
2090	-14 8 1 1400.97 174.807 5
2091	-14 8 2 723.000 126.165 5
2092	-14 9 -1 547.173 128.762 5
2093	-14 9 0 332.424 114.591 5
2094	-14 9 1 528.093 112.418 5
2095	-14 9 2 33.4821 70.2592 5
2096	-14 10 0-67.4512 70.7662 5
2097	-14 10 1 353.542 77.7588 5
2098	15 0 -2 187.330 211.906 7
2099	15 0 -1 607.210 248.260 7
2100	15 0 -1 23.3497 150.560 6
2101	15 0 0-113.735 134.934 6
2102	15 0 0 737.358 277.208 7
2103	15 0 1-25.6912 122.333 6
2104	15 0 2 83.3781 120.166 6
2105	15 0 3 50.8231 137.370 6
2106	15 0 4-20.1232 109.839 6
2107	15 -1 -4 2789.83 199.276 3
2108	15 1 -2 5173.86 704.085 7
2109	15 -1 -1 5818.97 372.269 6
2110	15 1 -1 5749.10 376.371 6
2111	15 1 -1 4996.79 598.165 7
2112	15 1 0 1977.20 221.930 6
2113	15 -1 0 1843.38 213.558 6
2114	15 1 0 1521.48 366.946 7
2115	15 -1 1 5951.21 342.282 6
2116	15 1 1 6069.67 345.942 6
2117	15 -1 2 6030.29 348.278 6
2118	15 1 2 6386.19 364.375 6
2119	15 -1 3 3005.29 268.822 6
2120	15 1 3 2763.93 267.221 6
2121	15 -1 4 2464.74 215.178 6
2122	15 1 4 2155.14 208.901 6
2123	15 -2 -4 4669.38 239.332 3
2124	15 2 -2 1957.41 458.997 7
2125	15 2 -1 1679.55 385.659 7
2126	15 -2 -1 1621.78 234.639 6
2127	15 2 -1 1534.13 220.113 6
2128	15 -2 0 383.328 137.769 6
2129	15 2 0 428.304 142.706 6
2130	15 2 0 647.920 299.651 7
2131	15 2 1 1562.83 196.752 6
2132	15 -2 1 1529.59 193.328 6
2133	15 -2 2 1983.00 210.251 6
2134	15 2 2 2310.41 238.693 6
2135	15 -2 3 792.409 156.110 6
2136	15 2 3 610.688 163.282 6
2137	15 -2 4 3974.70 231.194 6
2138	15 2 4 4035.29 265.516 6
2139	15 -3 -4 1913.67 153.831 3
2140	15 3 -2 5514.96 677.747 7
2141	15 3 -1 2457.26 458.544 7
2142	15 -3 -1 2935.87 281.950 6
2143	15 3 -1 2716.16 280.725 6
2144	15 -3 0 3113.21 265.031 6
2145	15 3 0 3104.99 267.096 6
2146	15 3 0 3161.41 481.214 7
2147	15 -3 1 2790.81 239.771 6
2148	15 3 1 2594.56 237.430 6
2149	15 3 2 5794.02 344.173 6
2150	15 3 3 398.724 144.926 6
2151	15 3 4 3753.82 230.810 6
2152	15 4 -1 878.882 190.876 6
2153	15 4 -1 1330.79 340.154 7
2154	15 4 0 261.681 151.475 6
2155	15 4 0 424.049 266.272 7
2156	-15 4 1 932.793 165.288 5
2157	15 4 1 656.623 161.356 6
2158	15 4 2 58.5214 114.576 6
2159	15 4 3 989.310 163.286 6
2160	15 4 4 1232.75 132.900 6
2161	15 5 0 16844.5 1157.03 7
2162	-15 5 1 558.674 158.905 5
2163	15 5 1 331.503 128.964 6
2164	-15 5 2 854.437 158.632 5
2165	15 5 2 751.122 158.639 6
2166	15 5 3 1290.15 158.210 6
2167	15 5 4 249.306 66.6615 6
2168	-15 6 0 4493.14 283.236 5
2169	-15 6 1 1241.58 191.645 5
2170	-15 6 2 667.309 157.820 5
2171	-15 7 -2 169.845 113.074 5
2172	-15 7 -1 294.924 137.829 5
2173	-15 7 0 4139.77 273.406 5
2174	-15 7 1 131.616 128.302 5
2175	-15 7 2 170.145 108.288 5
2176	-15 8 -2 1272.98 129.814 5
2177	-15 8 -1 970.151 154.312 5
2178	-15 8 0 52.6381 113.335 5
2179	-15 8 1 1293.16 161.585 5
2180	-15 8 2 1775.04 156.190 5
2181	-15 9 -1 779.457 119.105 5
2182	-15 9 0 238.160 102.302 5
2183	-15 9 1 674.624 106.150 5
2184	-15 9 2 360.160 81.0867 5
2185	-15 10 0 120.747 63.7522 5
2186	16 0 -1 12136.0 543.684 6
2187	16 0 -1 12539.8 895.261 7
2188	16 0 0 2810.42 271.550 6
2189	16 0 1 12768.8 512.786 6
2190	16 0 2 51.4559 126.419 6
2191	16 0 3 8856.37 432.802 6
2192	16 0 4 82.3569 113.965 6
2193	16 1 -2 113.644 201.272 7
2194	16 -1 -1 828.894 185.801 6
2195	16 1 -1 486.608 174.717 6
2196	16 1 -1 785.203 316.281 7
2197	16 -1 0 323.667 149.775 6
2198	16 1 0 379.536 163.351 6
2199	16 1 0 12.3865 216.868 7
2200	16 -1 1 718.717 163.517 6
2201	16 1 1 558.725 165.067 6
2202	16 -1 2 739.406 163.528 6
2203	16 1 2 794.898 175.237 6
2204	16 -1 3 2583.83 249.450 6
2205	16 1 3 2574.15 260.673 6
2206	16 -1 4 736.817 134.779 6
2207	16 1 4 1060.57 159.544 6
2208	16 -2 -1 3312.98 302.278 6
2209	16 2 -1 3070.97 303.188 6
2210	16 2 -1 3513.87 535.371 7
2211	16 -2 0 3179.70 273.233 6
2212	16 2 0 2843.96 264.195 6
2213	16 2 0 2384.24 464.775 7
2214	16 -2 1 3099.92 267.223 6
2215	16 2 1 3263.66 276.719 6
2216	16 -2 2 957.200 173.807 6
2217	16 2 2 1076.79 190.457 6
2218	16 -2 3 513.914 141.580 6
2219	16 2 3 300.538 145.927 6
2220	16 -2 4 669.285 109.776 6
2221	16 2 4 654.764 129.171 6
2222	16 -3 -1 1541.92 238.917 6
2223	16 3 -1 1200.19 218.453 6
2224	16 3 -1 1068.26 380.976 7
2225	16 -3 0-174.566 150.561 6
2226	16 3 0 50.6976 132.881 6
2227	16 3 0-49.1839 221.221 7
2228	16 -3 1 1201.74 181.512 6
2229	16 3 1 1436.48 201.980 6
2230	16 3 2 1793.71 222.876 6
2231	16 3 3 2532.51 238.715 6
2232	16 3 4 1510.58 155.960 6
2233	16 4 -1 2042.07 242.924 6
2234	16 4 0 1882.45 233.052 6
2235	16 4 0 2079.90 461.757 7
2236	16 4 1 2223.72 235.877 6
2237	-16 4 1 2281.86 222.865 5
2238	16 4 2 1424.07 194.573 6
2239	16 4 3 1058.39 164.885 6
2240	16 4 4 1266.55 125.596 6
2241	16 5 1 2117.69 226.034 6
2242	-16 5 1 2448.69 235.301 5
2243	-16 5 2 204.748 128.334 5
2244	16 5 2 123.579 107.393 6
2245	16 5 3 1178.76 144.765 6
2246	-16 6 0 199.289 133.874 5
2247	-16 6 1 795.546 163.658 5
2248	-16 6 2 288.013 135.448 5
2249	-16 7 -2 266.391 113.612 5
2250	-16 7 -1 3689.30 253.384 5
2251	-16 7 0 17.8567 126.234 5
2252	-16 7 1 4097.79 266.590 5
2253	-16 7 2 260.895 103.790 5
2254	-16 8 -2 129.842 71.9665 5
2255	-16 8 -1 1738.57 177.643 5
2256	-16 8 0 1105.20 157.288 5
2257	-16 8 1 1393.83 155.139 5
2258	-16 8 2 84.8703 88.3333 5
2259	-16 9 -1 212.758 89.0001 5
2260	-16 9 0 123.246 92.0808 5
2261	-16 9 1 252.463 83.3338 5
2262	17 0 -1-158.911 182.612 6
2263	17 0 0-18.0679 142.336 6
2264	17 0 1 138.542 142.302 6
2265	17 0 2-49.7488 133.820 6
2266	17 0 3-9.69558 118.428 6
2267	17 0 4 114.800 97.0154 6
2268	17 -1 -1 4422.70 364.867 6
2269	17 1 -1 4426.54 367.288 6
2270	17 1 -1 3514.64 565.193 7
2271	17 -1 0 8132.85 443.177 6
2272	17 1 0 7939.68 436.760 6
2273	17 -1 1 4269.20 323.702 6
2274	17 1 1 4735.58 335.789 6
2275	17 -1 2 6933.65 382.193 6
2276	17 1 2 6337.67 375.675 6
2277	17 -1 3 374.242 141.887 6
2278	17 1 3 146.040 137.303 6
2279	17 -1 4 1248.58 145.835 6
2280	17 1 4 1257.26 154.098 6
2281	17 -2 -1 1391.44 231.547 6
2282	17 2 -1 1005.39 223.954 6
2283	17 2 -1 1261.41 397.850 7
2284	17 -2 0 2665.17 269.895 6
2285	17 2 0 2413.93 265.056 6
2286	17 2 0 2447.13 487.180 7
2287	17 -2 1 1413.34 201.129 6
2288	17 2 1 1070.60 191.951 6
2289	17 -2 2 508.884 153.035 6
2290	17 2 2 398.055 156.851 6
2291	17 -2 3 1014.29 160.904 6
2292	17 2 3 463.306 142.581 6
2293	17 2 4-77.2747 93.8562 6
2294	17 -3 -1 2021.14 257.605 6
2295	17 3 -1 2158.74 277.618 6
2296	17 -3 0-25.8021 146.710 6
2297	17 3 0 171.718 142.200 6
2298	17 3 0-164.983 259.304 7
2299	17 -3 1 2151.35 238.610 6
2300	17 3 1 2049.66 231.749 6
2301	17 -3 2 3071.79 255.537 6
2302	17 3 2 2910.12 268.357 6
2303	17 3 3 2208.69 218.815 6
2304	17 3 4 1013.90 124.969 6
2305	17 4 -1 1534.74 235.403 6
2306	17 4 0 717.321 182.670 6
2307	17 4 1 1299.56 205.657 6
2308	-17 4 1 1527.19 205.293 5
2309	17 4 2 226.553 125.017 6
2310	17 4 3 3120.81 229.186 6
2311	17 4 4 685.686 86.6717 6
2312	17 5 1 1473.83 197.970 6
2313	-17 5 1 1677.31 200.895 5
2314	17 5 2-251.803 116.559 6
2315	17 5 3 359.539 101.448 6
2316	-17 6 0-48.8259 114.839 5
2317	-17 6 1-40.5557 127.582 5
2318	-17 6 2 1588.86 181.040 5
2319	-17 7 -2 296.584 105.011 5
2320	-17 7 -1 1192.45 173.785 5
2321	-17 7 0 2404.80 214.259 5
2322	-17 7 1 1040.32 156.453 5
2323	-17 7 2 370.907 111.015 5
2324	-17 8 -1 1272.52 155.014 5
2325	-17 8 0 1643.26 176.304 5
2326	-17 8 1 1306.61 146.086 5
2327	-17 9 0 244.800 89.7443 5
2328	-17 9 1 188.430 70.2492 5
2329	18 0 -1 5747.15 415.454 6
2330	18 0 0 59.3955 156.978 6
2331	18 0 1 5700.22 384.404 6
2332	18 0 2 4572.79 327.291 6
2333	18 0 3 1827.31 219.437 6
2334	18 0 4 816.060 125.988 6
2335	18 -1 -1 935.882 226.582 6
2336	18 1 -1 742.742 226.763 6
2337	18 1 -1 1138.19 379.482 7
2338	18 -1 0 269.230 175.526 6
2339	18 1 0 78.4529 141.692 6
2340	18 -1 1 1039.86 196.315 6
2341	18 1 1 1349.36 218.601 6
2342	18 -1 2 2185.42 240.704 6
2343	18 1 2 2215.71 241.906 6
2344	18 -1 3 869.190 166.703 6
2345	18 1 3 924.681 173.612 6
2346	18 1 4 1180.88 135.164 6
2347	18 -1 4 1143.69 124.083 6
2348	18 -2 -1 3575.94 325.772 6
2349	18 2 -1 3144.95 320.173 6
2350	18 -2 0-39.3846 159.440 6
2351	18 2 0-95.2172 149.527 6
2352	18 -2 1 3777.57 303.999 6
2353	18 2 1 3915.14 311.323 6
2354	18 -2 2 1482.47 197.801 6
2355	18 2 2 1401.01 206.174 6
2356	18 -2 3 687.099 145.816 6
2357	18 2 3 686.177 153.159 6
2358	18 2 4 241.955 87.1400 6
2359	18 -3 -1 1098.75 214.928 6
2360	18 3 -1 1115.83 231.613 6
2361	18 -3 0 5133.35 356.086 6
2362	18 3 0 5206.67 367.968 6
2363	-18 3 1 1351.00 191.374 5
2364	18 -3 1 1405.74 207.921 6
2365	18 3 1 1135.51 197.812 6
2366	18 3 2 957.515 180.071 6
2367	18 3 3 2354.23 208.777 6
2368	18 3 4 110.487 64.3980 6
2369	18 4 -1 2484.74 276.272 6
2370	18 4 0 303.438 165.391 6
2371	18 4 1 2396.92 249.795 6
2372	-18 4 1 2508.98 228.897 5
2373	18 4 2 107.010 127.602 6
2374	18 4 3 169.939 104.664 6
2375	18 5 1 2964.08 257.190 6
2376	-18 5 1 3470.78 260.703 5
2377	18 5 2-48.6729 107.335 6
2378	18 5 3 498.064 99.6418 6
2379	-18 6 -2 30.0575 93.2835 5
2380	-18 6 -1 582.813 147.685 5
2381	-18 6 0 152.380 122.901 5
2382	-18 6 1 180.693 124.813 5
2383	-18 7 -2 630.009 110.044 5
2384	-18 7 -1 250.495 127.534 5
2385	-18 7 0 1594.90 182.547 5
2386	-18 7 1 283.932 118.991 5
2387	-18 7 2 247.204 87.7246 5
2388	-18 8 -1 162.104 98.2153 5
2389	-18 8 0 805.354 134.286 5
2390	-18 8 1 186.578 91.3486 5
2391	-18 9 0 51.6157 62.9025 5
2392	19 0 -1 59.9367 179.050 6
2393	19 0 0-62.7631 172.710 6
2394	19 0 1 51.0635 142.521 6
2395	19 0 2-7.37469 133.301 6
2396	19 0 3-135.645 129.489 6
2397	19 0 4-107.975 77.8456 6
2398	19 -1 -1 1243.42 245.451 6
2399	19 1 -1 1113.87 252.544 6
2400	19 -1 0 8030.48 473.536 6
2401	19 1 0 7852.59 461.195 6
2402	19 -1 1 1327.37 223.618 6
2403	19 1 1 1350.12 220.964 6
2404	19 -1 2 507.838 157.040 6
2405	19 1 2 412.559 146.717 6
2406	19 -1 3 193.273 115.295 6
2407	19 1 3 178.762 117.990 6
2408	19 1 4 637.743 99.4687 6
2409	19 -2 -1 1017.82 229.023 6
2410	19 2 -1 1045.35 229.664 6
2411	19 -2 0 81.2448 153.861 6
2412	19 2 0 186.090 162.193 6
2413	19 -2 1 1339.17 217.480 6
2414	19 2 1 951.403 201.288 6
2415	19 -2 2 579.927 160.469 6
2416	19 2 2 485.935 156.194 6
2417	19 -2 3 505.901 130.987 6
2418	19 2 3 436.348 139.056 6
2419	19 2 4 1196.18 115.170 6
2420	19 3 -1-125.465 174.077 6
2421	19 -3 0-58.0230 147.146 6
2422	19 3 0 376.225 176.440 6
2423	-19 3 1 238.787 155.738 5
2424	19 -3 1-127.134 150.422 6
2425	19 3 1 120.358 140.980 6
2426	19 3 2 149.040 128.747 6
2427	19 3 3 104.532 99.4119 6
2428	19 4 -1 991.599 205.209 6
2429	19 4 0 413.938 166.718 6
2430	-19 4 1 1363.07 198.037 5
2431	19 4 1 1071.55 188.450 6
2432	19 4 2 830.704 164.175 6
2433	19 4 3 54.6298 79.6207 6
2434	-19 5 -3 467.155 87.8183 5
2435	-19 5 0 139.108 120.796 5
2436	-19 5 1 515.278 156.294 5
2437	19 5 1 398.750 139.238 6
2438	19 5 2 1416.03 164.504 6
2439	19 5 3 382.186 76.6052 6
2440	-19 6 -2 604.690 122.926 5
2441	-19 6 -1 2006.43 199.758 5
2442	-19 6 0 190.356 128.368 5
2443	-19 6 1 1895.99 193.438 5
2444	-19 7 -2-0.73988 69.5962 5
2445	-19 7 -1 106.393 115.499 5
2446	-19 7 0 572.744 135.845 5
2447	-19 7 1 193.717 100.928 5
2448	-19 8 -1-35.0670 81.2789 5
2449	-19 8 0 1903.34 157.993 5
2450	-19 8 1 25.6634 67.7714 5
2451	20 0 -1 497.367 218.977 6
2452	20 0 0 13638.1 620.386 6
2453	20 0 1 984.381 210.834 6
2454	20 0 2 169.682 130.815 6
2455	20 0 3 451.307 136.008 6
2456	20 -1 -1 1712.44 280.507 6
2457	20 1 -1 992.912 221.830 6
2458	20 -1 0-149.988 177.813 6
2459	20 1 0-62.8270 170.975 6
2460	20 -1 1 1280.66 218.869 6
2461	20 1 1 1194.23 216.474 6
2462	20 -1 2 227.350 142.183 6
2463	20 1 2 203.418 140.969 6
2464	20 -1 3 510.720 134.888 6
2465	20 1 3 416.826 135.055 6
2466	20 -2 -1 217.459 170.076 6
2467	20 2 -1 97.9211 171.247 6
2468	20 -2 0 1363.81 235.173 6
2469	20 2 0 1139.73 218.735 6
2470	20 -2 1 179.978 161.922 6
2471	20 2 1 195.912 143.153 6
2472	20 -2 2 314.159 118.200 6
2473	20 2 2 206.804 146.256 6
2474	20 -2 3 725.242 127.146 6
2475	20 2 3 517.663 125.896 6
2476	20 3 -1 1102.22 213.170 6
2477	20 -3 0 165.714 151.249 6
2478	20 3 0 325.456 175.586 6
2479	20 -3 1 936.324 184.822 6
2480	20 3 1 1323.70 203.730 6
2481	20 3 2 219.023 129.705 6
2482	20 3 3 1383.43 153.794 6
2483	20 4 -1 624.332 176.761 6
2484	20 4 0 391.566 161.145 6
2485	-20 4 1 675.185 170.300 5
2486	20 4 1 602.690 156.605 6
2487	20 4 2 646.680 145.633 6
2488	20 4 3 472.134 89.5039 6
2489	-20 5 0 104.401 130.382 5
2490	-20 5 1 240.984 132.481 5
2491	20 5 1-24.2943 127.485 6
2492	20 5 2 219.224 100.278 6
2493	-20 6 -2 127.378 87.7500 5
2494	-20 6 -1 252.087 120.936 5
2495	-20 6 0 1276.87 172.711 5
2496	-20 6 1 122.784 119.698 5
2497	-20 7 -1 348.314 112.655 5
2498	-20 7 0 272.559 110.998 5
2499	-20 7 1 207.846 95.0047 5
2500	-20 8 0 209.342 74.0750 5
2501	21 0 -1-81.4510 163.925 6
2502	21 0 0 45.1196 184.626 6
2503	21 0 1-89.4242 147.628 6
2504	21 0 2 31.6520 121.540 6
2505	21 0 3-78.6381 104.281 6
2506	21 -1 -1 2218.22 285.009 6
2507	21 1 -1 1820.40 267.064 6
2508	21 -1 0 1018.06 223.181 6
2509	21 1 0 1037.90 222.642 6
2510	21 -1 1 1852.80 242.083 6
2511	21 1 1 2173.38 262.710 6
2512	21 -1 2 203.768 128.740 6
2513	21 1 2 167.637 131.111 6
2514	21 -1 3 1268.22 155.936 6
2515	21 1 3 1406.12 165.288 6
2516	21 -2 -1 751.210 204.348 6
2517	21 2 -1 728.787 199.952 6
2518	21 -2 0 89.7231 162.802 6
2519	21 2 0 145.258 166.093 6
2520	21 -2 1 471.691 162.310 6
2521	21 2 1 738.579 174.390 6
2522	21 -2 2 628.147 147.103 6
2523	21 2 2 370.161 146.487 6
2524	21 2 3 433.984 114.580 6
2525	21 3 -1 356.073 168.009 6
2526	21 -3 0 283.379 146.824 6
2527	21 3 0 114.849 154.816 6
2528	21 -3 1 206.730 135.178 6
2529	21 3 1 316.371 147.590 6
2530	21 3 2 162.561 116.193 6
2531	21 3 3 169.281 84.5099 6
2532	21 4 0 61.1064 125.261 6
2533	-21 4 1 967.766 198.445 5
2534	21 4 1 477.547 150.053 6
2535	21 4 2 612.663 134.555 6
2536	-21 5 0 126.216 118.614 5
2537	-21 5 1 962.418 169.209 5
2538	21 5 1 410.267 128.145 6
2539	21 5 2-94.4028 80.6166 6
2540	-21 6 -2 107.094 70.8640 5
2541	-21 6 -1-21.7954 98.8702 5
2542	-21 6 0 26.1729 112.256 5
2543	-21 6 1 44.9814 104.636 5
2544	-21 7 -1 318.243 90.1040 5
2545	-21 7 0 228.083 98.2796 5
2546	22 0 -1 1264.58 232.284 6
2547	22 0 0 7962.38 459.478 6
2548	22 0 1 1305.96 210.530 6
2549	22 0 2 3439.12 270.955 6
2550	22 0 3 61.7587 90.1839 6
2551	22 -1 -1 410.941 184.830 6
2552	22 1 -1 541.671 193.094 6
2553	22 -1 0 422.149 179.093 6
2554	22 1 0 514.288 184.178 6
2555	22 -1 1 476.537 168.354 6
2556	22 1 1 564.584 174.955 6
2557	22 -1 2 187.993 118.433 6
2558	22 1 2 200.807 129.114 6
2559	22 -1 3 122.990 86.8083 6
2560	22 1 3 154.904 86.9693 6
2561	22 2 -1 83.5078 144.879 6
2562	22 -2 0 2743.35 265.053 6
2563	22 2 0 2678.86 273.359 6
2564	22 -2 1 9.88577 133.125 6
2565	22 2 1 184.253 137.132 6
2566	22 -2 2 338.191 113.361 6
2567	22 2 2 572.820 145.290 6
2568	22 2 3 237.216 85.7496 6
2569	22 -3 0 745.655 165.238 6
2570	22 3 0 626.969 163.599 6
2571	22 -3 1 864.277 159.200 6
2572	22 3 1 1135.87 184.276 6
2573	22 3 2 395.148 127.391 6
2574	-22 4 0-138.350 124.215 5
2575	22 4 0 120.042 129.887 6
2576	22 4 1 738.756 158.279 6
2577	22 4 2 997.058 133.912 6
2578	-22 5 -2 150.659 76.9628 5
2579	-22 5 -1 410.601 116.742 5
2580	-22 5 0 944.081 154.974 5
2581	-22 6 -1 111.791 90.7929 5
2582	-22 6 0 275.397 113.407 5
2583	23 0 -1 269.866 162.071 6
2584	23 0 0-75.8142 163.594 6
2585	23 0 1-177.132 153.973 6
2586	23 0 2 41.2240 111.331 6
2587	23 1 -1 813.907 197.184 6
2588	23 -1 0 584.121 183.587 6
2589	23 1 0 350.484 171.322 6
2590	23 -1 1 567.668 148.221 6
2591	23 1 1 374.120 154.702 6
2592	23 -1 2 456.602 128.785 6
2593	23 1 2 730.883 143.887 6
2594	23 -2 0 356.376 151.553 6
2595	23 2 0 142.677 148.819 6
2596	23 -2 1 300.718 139.292 6
2597	23 2 1 143.417 117.968 6
2598	23 -2 2 830.896 132.142 6
2599	23 2 2 810.200 145.681 6
2600	-23 3 0 170.506 132.932 5
2601	23 3 0 153.807 123.187 6
2602	23 3 1 1909.11 207.173 6
2603	23 3 2 51.9950 91.0072 6
2604	-23 4 0 305.586 125.835 5
2605	23 4 0 73.9292 106.250 6
2606	23 4 1 119.058 101.716 6
2607	23 4 2 79.9693 69.2771 6
2608	-23 5 -1 848.391 116.967 5
2609	-23 5 0 194.885 111.042 5
2610	24 0 0 1708.17 217.200 6
2611	24 0 1 934.377 173.879 6
2612	24 0 2 534.103 120.246 6
2613	24 -1 0 999.062 185.511 6
2614	24 1 0 719.550 177.723 6
2615	24 -1 1 1142.82 176.466 6
2616	24 1 1 1291.04 181.603 6
2617	24 -1 2 267.893 103.579 6
2618	24 1 2 396.159 107.784 6
2619	24 -2 0 7.60727 118.584 6
2620	24 2 0 98.0194 136.373 6
2621	24 -2 1-12.0932 99.9097 6
2622	24 2 1-44.0626 116.342 6
2623	24 2 2 83.5721 88.6742 6
2624	-24 3 0-120.133 126.196 5
2625	24 3 0 91.1937 108.701 6
2626	24 3 1 915.094 145.763 6
2627	24 3 2 141.774 74.0342 6
2628	-24 4 -1 19.9049 83.4347 5
2629	-24 4 0 162.620 111.298 5
2630	24 4 1-3.57402 79.5485 6
2631	25 0 0 38.9353 126.196 6
2632	25 0 1 2.57605 104.148 6
2633	25 -1 0 315.222 129.714 6
2634	25 1 0 126.613 115.273 6
2635	25 -1 1 539.682 130.314 6
2636	25 1 1 538.625 127.813 6
2637	25 1 2 605.716 98.6754 6
2638	25 2 0 135.022 107.523 6
2639	25 -2 1 664.744 106.201 6
2640	25 2 1 870.311 139.513 6
2641	-25 3 -1 68.8367 77.7697 5
2642	25 3 0 106.124 91.2146 6
2643	25 3 1 89.1986 82.6922 6
2644	26 0 1 87.5328 76.8157 6
2645	26 1 1 302.669 91.8059 6
2646	0 0 0 0.00 0.00 0
2647
2648	TITL JH1902b in Pca2(1)
2649	REM Pca2(1) (#29, found as P2(1)ca in -cba setting)
2650	CELL 1.54184 21.499126 9.804085 4.768275 90.0000 90.0000 90.0000
2651	ZERR 4.00 0.002078 0.000872 0.000349 0.0000 0.0000 0.0000
2652	LATT -1
2653	SYMM -x,-y, z+1/2
2654	SYMM x+1/2,-y, z
2655	SYMM -x+1/2, y, z+1/2
2656	SFAC C H N O
2657	UNIT 24.00 60.00 12.00 24.00
2658	TREF
2659	HKLF 4
2660	END
2661	;
2662	_shelx_hkl_checksum 50030
2663
2664	#===END
2665

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